Synthesis and Characterizations of Ni-W alloy

Potdar, Dipali; Patil, Sushant; Kulkarni, Yugen; Pawar, Niketa; Sadale, Shivaji; CHIKODE, PRASHANT

doi:10.22068/ijmse.3535

Volume 21, Issue 1 (March - Special Issue 2024) IJMSE 2024, 21(1): 51-55 | Back to browse issues page

‎ 10.22068/ijmse.3535

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Potdar D, Patil S, Kulkarni Y, Pawar N, Sadale S, CHIKODE P. Synthesis and Characterizations of Ni-W alloy. IJMSE 2024; 21 (1) :51-55
URL: http://ijmse.iust.ac.ir/article-1-3535-en.html

Synthesis and Characterizations of Ni-W alloy

Dipali Potdar

Abstract: (6104 Views)

The Nickel tungsten (Ni-W) alloy was electrodeposited on stainless steel (SS) substrate using potentiostatic mode at room temperature. Potentiostatic electrodeposition was carried out by varying the deposition time. The physicochemical properties of Ni-W alloys were studied using X-Ray diffraction (XRD), Electron Microscopy and micro-Raman spectroscopy. Recorded XRD spectra was compared with standard JCPDS card and the presence of Ni was confirmed, no such peaks for W were observed. Further study was extended for micro-Raman analysis. From Raman spectroscopy study the appearance of Ni-O and W⁶⁺=O bonds confirms that the Ni-W present in amorphous phase. Several cracks were observed in SEM images along with nanoparticles distributed over the electrode surface. The appearance of cracks may be correlated with the in-plane tensile stresses, lattice strains and stacking faults and may be related to the substrate confinements.

Keywords: Ni-W, Alloy, Electrodeposition, Amorphous, Raman Spectroscopy.